Alloy Nanoparticle UHV Deposition Source: NL-UHV Series

Deposit pure and alloy nanoparticles with precise control over size and composition

Nanoparticles for functional coatings

The NL-UHV Series are nanoparticle deposition sources that deposit pure and alloy nanoparticles in ultra-high vacuum onto your sample, creating functional coatings. Moreover, we can customize the properties of nanoparticle coatings by precisely controlling the size, composition, and structure of the nanoparticles. Furthermore, the NL-UHV is available with  the following sources: a single 1” source (NL-D1), a 2” source (NL-D2), or a triple 1” source (NL-D3). Lastly, we can integrate these sources into your existing PVD systems or incorporate them into our custom-built NEXUS and NL-FLEX vacuum system.

Key Features

  • Deposit pure and alloy, hydrocarbon-free, non-agglomerated nanoparticles.
  • Achieve sub-monolayer or high-porosity 3-D nanocoating.
  • The NL-D3 facilitates the deposition of up to three materials, either individually or as alloys, using two or three materials at the same time.
  • All sources are compatible with both DC and Pulsed DC power supplies.
  • Control the properties of the nanoparticle coatings by adjusting various process parameters, such as gas flow, gas type, magnetron power, and aggregation length (Lg), or by altering the size of the aggregation zone aperture.

Control of Nanoparticle size using NL- QMS
Quadrupole Mass Spectrometer

The NL-QMS mass filter enables real-time scanning or filtering of deposited nanoparticles by mass or diameter, facilitating the optimization of growth conditions.

Highlights

⇒ Adjust the nanoparticle size distribution within the range of 1 – 20 nm.

⇒ Modify the nanocoating layer density from a sub-monolayer to 3D nanoporous coverage, facilitating coatings that range from loosely bound to tightly adherent.

⇒ Manage the nanoparticle shape and structure, transitioning from crystalline to amorphous forms.

⇒ Conduct mass spectrum analysis of nanoparticles in flight, covering a range from 100 – 10 6 amu.

⇒ Implement nanoparticle size filtering with a mass resolution accuracy of +/-2%.

NL- QMS Control Software

QMS software

The NL-QMS  is operated through a simple and user-friendly Windows™ software interface.

Highlights

  • Data logging for mass spectra

  • Preloaded mass calibration data for standard materials

  • Input parameters for novel materials or alloys

  • Complete control over QMS operations and scanning configurations

Specifications

UtilityNL-DXXNL-QMS
Mounting FlangeDN160CFDN160CF
Power630V DC or Pulsed DC100-250Vac
4Amp fuse
GasArgon/Helium
2-100Sccm
Cooling JacketWater or LN2
Flow rate 2l/min (0.52 US GPM)
Pumping120L/m (4.2 CFM) Backing pump
300L/m (10.6 CFM) Turbo pump
Aperture plates2mm, 3mm, 4mm and 5mm aperture plates
supplied as standard

NL-DXX Options

Source OptionsNL-D1NL-D2NL-D3
Source Output75W dc100W dc3 x 75W dc
Sputter Target1 x 1″1 x 2″3 x 1″
Target Thickness0.5 – 3mm
NL-UHV Tech Note
AP02 HEA nanoparticles as OER catalysts for Green Hydrogen
Read more..

Publications

Elizabeth S. Jones, Dr. Charalampos Drivas, Dr. Joshua S. Gibson, Dr. Jack E. N. Swallow, Dr. Leanne A. H. Jones, Thomas D. J. Bricknell, Dr. Matthijs A. van Spronsen, Prof. Georg Held, Dr. Mark A. Isaacs, Dr. Christopher M. A. Parlett, Prof. Robert S. Weatherup.  DOI: 10.1002/cctc.202400239

Florian Knabl, Dominik Gutnik, Prathamesh Patil, Christine Bandl, Tijmen Vermeij, Christian M. Pichler, Barbara Putz, Christian Mitterer. DOI:10.1016/j.vacuum.2024.113724

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